DIRECTORATE GENERAL NATIONAL SECURITY GUARD OPERATIONS BRANCH (WE SEC) 1. Formulation of QRs for Mobile Chemical Detection Lab as per Appx att are being contemplated. 2. OEM/Firms are requested to forward their comments/suggestions on the draft QRs as per proforma given below alongwith the details (product specifications, pectoral’s etc) of their product meeting the referred QRs. 3. It is requested that comments if any on the QRs may please be forwarded to the under mentioned within 30 days. Operations Directorate WE Branch HQ National Security Guard Mehram Nagar Near Domestic Airport Palam New Delhi – 110037 Fax No – 011-25671528++ E-mail : twoic.weops@nsg.gov.in DRAFT QRs OF MOBILE CHEMICAL DETECTION LAB Ser No 1 1. 2 3 Draft QR Vendor Comments 2 The GC/MS system must be supplied as a complete kit. The kit will include a GC/MS, desired sampling tools, selected spare parts kits, and a standard laptop Dimensions. Notwith Exceeding installed20x20x22 operatinginches. software, test methods, and spectral libraries. Weight. Not Exceeding 50 Kgs including all accessories. 3 4 GC/MS must have mass range of at least 50 to 400 m/z and be capable of up to 10,000 m/z per second @ 20 points per m/z including the ability to acquire full-scan or Single Ion Monitoring (SIM) data. 5 6 The GC column must be of Low-Thermal Mass (LTM). The LTM-GC must be temperature programmable from 50°C to 300°C, with at least 300°C maximum temperature and a temperature ramp rate of up to 90°C/min. GC/MS must preferably accept multiple power source options, including input voltage of 100–120/220–240 VAC, 50/60 Hz, and 15 A. It may also be powered by 24 VDC C (+/- 5%, 25 A, 600 W) via external or battery source and provide a fuse protection (30 A minimum). GC/MS should preferably provide two non-coated inert electron ionization (EI) sources for interchangeable ion volumes and to facilitate rapid change out of ‘dirty source’. 7 8 2 Ser No 1 9 Draft QR Vendor Comments 2 GC/MS system must contain a completely integrated vacuum pump system. GC/MS must NOT require external pumping or vacuum modified devices. 3 10 GC/MS must be able to power up, pump down, and reach appropriate temperature within 30 minutes of startup, as well as be capable of warm up/pump down during transit. 11. GC/MS must be ruggedized for mobile applications(outside of a laboratory), including integrated wire rope isolators. Must have passed MIL-STD-810G, Method 514.6, Table 514.6C-II Category 4. 12. The GC/MS system must provide both an integrated split/split-less standard injector port (SIP) and integrated universal sampling port (USP) for plug and play samplers. External accessories will not be accepted. GC/MS must provide connection for external helium (He) gas cylinder or Hydrogen (H2) generator. The GC/MS should not utilize proprietary carrier gas canisters. 13. 14. GC/MS must utilize an on-board calibrant that is non-proprietary. 15. GC/MS system must preferably be able to condition one smart sampler for re-use while desorbing samples from a second smart sampler for analysis. 16. Software should preferably be capable of pre-programming sample collection methods for the smart sampler including time- and volumebased sample collection methods, as well as manual collection options. 3 Ser No 1 17. Draft QR Vendor Comments 2 3 GC/MS software should provide both qualitative and quantitative sample analysis. 18. Software should be capable of Sequential Full Scan/SIM acquisitions to acquire full scan and SIM data in a single injection including centroid or profile data acquisition with at least 15 samples/amu. 19. User interface should preferably offer a wizard to guide users through a step-by-step interactive Q&A, enabling them to select the most applicable test method for their application. 20. GC/MS system should operate using system software offering at least 2 user-interfaces: Operator and Developer. The GC/MS software must be supplied with both a simplified user interface and advanced user interface. The simplified user interface should be able to be learned within 8 hours of instruction and should include a wizard for assistance in selecting the appropriate test method. The advanced user interface will provide the ability to develop custom libraries and methods, as well as provide advanced programming for the simplified user interface. Both interfaces will have security level access through password coded protection. The system must accept solid, liquid, and vapor samples via a complete suite of sample introduction tools. The sampling tools must include options for both prepared and native samples. The GC/MS must be compatible with a number of optional sample introduction tools including: manual syringe injections, auto-sampler injections, manual headspace syringe, solid phase micro extraction (“SPME”) fibers, air sampling adaptor for 24/7 sampling lines, handheld vapor sampler, purge and trap accessory, and the Prep-less Sample Introduction Probe (PSI-Probe). Each sampling method will be initiated by automated software and/or manual methods. 21. 22. 23. 4 Ser No 1 24. Draft QR Vendor Comments 2 The Universal Sampling Port (USP) should preferably be compatible with the following Plug and Play samplers for sample introduction: 3 (a) GC/MS system should include a sampling adaptor for 24/7 direct air intake through a sampling line. This adaptor will plug directly into the USP. No sample preparation should be required. (b) GC/MS system should be able accept vapor samples collected by the optional smart sampler accessory. The smart sampler plugs directly into the USP. No sample preparation should be required. (c) GC/MS system should accept water samples through the optional purge and trap accessory. This accessory should be compatible and plug directly into the USP. No sample preparation should be required. 25. 26. The system must include basic operational test methods, as well as spectral libraries that include a broad range of chemical targets. These spectral libraries must include explosives, narcotics, designer drugs, toxic industrial compounds (TICs), chemical warfare agents (CWAs), and other volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs). The system will also allow users to develop custom libraries and test methods that meet new materials of interest over time. The GC/MS and other selected accessories must be provided with custom built protective traveling cases. 5 Ser No 1 27. Mobile Platform Draft QR Vendor Comments 2 3 (i) The Mobile platform would be based on an air conditioned BS4 utility vehicle as per the laid down DG S&D rate contract. (ii) As per the requirement the following two utility vehicles based on BS4 platform have been shortlisted :(a) TATA Innova 2.5 E diesel 7 str BS4 PS AC (Rate contract and tech data att as per Appx A, A1). (b) TATA Sumo Gold LX (BS4) stg cap.8 (Opt.6+D) Rate contract and tech date att as per Appx B, B1) (iii) Mobile platform to be procured and modified by the firm in order to accommodate the Mobile Chemical Detection Lab. 28. Miscellaneous. (a) This whole package must be delivered with a full one year basic manufacturer’s warranty. (b) The option for on-site Operator and Certification must be available for up to 10 users. (c) Manufacturer must also Agreements for up to 3 years. offer optional Developer Service
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